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<div>　　總磷檢測在各種水質(zhì)監(jiān)測和處理中非常重要，一般采用總磷測定儀，測量原理主要采用國家標(biāo)準(zhǔn)：GB1183-89鉬酸銨分光光度法，檢測快速、安全、準(zhǔn)確、穩(wěn)定，是水質(zhì)總磷檢測、監(jiān)測的分析標(biāo)準(zhǔn)。總磷測定儀測總磷時(shí)會(huì)遇到的問題匯總分析如下：</div><div>　　1、水質(zhì)檢測儀測總磷時(shí)，如果水樣是強(qiáng)酸性或強(qiáng)堿性，會(huì)不會(huì)對實(shí)驗(yàn)產(chǎn)生影響？</div><div>　　總磷消解需要在中性條件下，操作方法是用10%稀硫酸或10%氫氧化鈉溶液調(diào)節(jié)成中性。中和時(shí)加入少量中和試劑，避免過度調(diào)節(jié)。</div><div>　　2、用水質(zhì)分析儀測量總磷，空白呈藍(lán)色。</div><div>　　空白呈藍(lán)色一般有兩種情況，一是硫酸含磷引起的空白呈藍(lán)色；二是蒸餾水污染，含磷呈藍(lán)色。</div><div>　　3、原水樣有顏色對總磷檢測結(jié)果有影響嗎？</div><div>　　若水樣消解后無顏色，則對檢測結(jié)果無干擾。水中的彩色物質(zhì)在消解過程中會(huì)消解成無色物質(zhì)，不影響測量結(jié)果。若水樣消解后有顏色，可采用濁度-色度補(bǔ)償?shù)姆椒y定。</div><div>　　4、加入試劑后，水樣不顯色。</div><div>　　此時(shí)水樣不顯色一般有如下三個(gè)原因一是水中不含磷，二是試劑失效，三是</div><div>　　將蒸餾水誤認(rèn)為水樣，或加錯(cuò)試劑。</div><div>　　5、測量總磷時(shí)，藍(lán)色物質(zhì)吸附在比色皿壁或沉淀在比色皿底部。</div><div>　　樣品放置時(shí)間過長，應(yīng)在反應(yīng)結(jié)束后30分鐘內(nèi)盡快確定，吸附或沉淀不利于比色皿的清洗。</div><div>　　6、測量數(shù)據(jù)不準(zhǔn)確</div><div>　　有干擾物質(zhì)存在，操作是否正確，曲線選擇是否正確，重新選擇或重新校準(zhǔn)曲線。</div> 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